Synthesis, characterization and properties of Mn-doped ZnO nanocrystals

Tóm tắt

In this work ZnO and Mn-doped ZnO nanocrystals were synthesized by one-step aqueous solution method. X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive x-ray (EDX) analysis and photoluminescence (PL) spectroscopy have been used to characterize the samples in detail. The XRD studies revealed that the ZnO and Mn-doped ZnO had wurtzite structure (hexagonal). The composition analysis by EDX indicated the presence of small amounts of Mn. A strong and wide ultraviolet emission has been observed for the ZnO and Mn-doped ZnO nanocrystals as evidenced by the photoluminescence spectra at a wavelength of 384 and 389 nm respectively. As-synthesized ZnO and Mn-doped ZnO nanocrystals have a good crystal quality. ZnO and Mn-doped ZnO nanocrystals show diamagnetism at room temperature.

Tài liệu tham khảo

[1] Pan Z W, Dai Z R and Wang Z L 2001 Science 291 1947

[2] Huang M H, Mao S, Feick H, Yan H, Wu Y, Kind H, Weber E, Russo R and Yang P 2001 Science 292 1897

[3] Meyer B K et al 2004 Physica Status Solidi B 241 231

[4] Madelung O (ed) 1992 Data in Science and Technology: Semiconductors (Berlin: Springer)

[5] Chen Y, Bagnall D and Yao T 2000 Mater. Sci. Eng. B 75 190

[6] Dayan N J, Sainkar S R, Karekar R N and Aiyer R C 1998 Thin Solid Films 325 254

[7] Saito N, Haneda H, Sekiguchi T, Ohashi N, Sakaguchi L and Koumoto K 2002 Adv. Mater. 14 418

[8] Chopra K L and Das S R 1983 Thin Film Solar Cells (New York: Plenum) 321

[9] Salam S, Islam M, Alam M, Akram A, Ikram M, Mahmood A, Khan M and Mujahid M 2011 Adv. Nature Sci.: Nanosci. Nanotechnol. 2 045001

[10] Hung N T, Quang N D and Bernik S 2001 Mater. Res. 16 2817

[11] Chieng D T, Long P D, Lam N H and Hoi P V 2010 Adv. Nature Sci.: Nanosci. Nanotechnol. 1 035010

[12] Dong L F, Cui L Z and Zhang Z K 1997 Nanostruct. Mater. 8 815

[13] Wu J J and Liu S C 2002 Adv. Mater. 14 215

[14] Yang P D, Yan H Q, Mao S, Russo R, Johnso J, Saykally R, Morris N, Pham J R, He R and Choj H J 2002 Adv. Funct. Mater. 12 323

[15] Kong Y C, Yu D P, Zhang B, Fang W and Feng S Q 2001 Appl. Phys. Lett. 78 407

[16] Dai Y, Zhang Y, Li Q K and Nan C W 2002 Chem. Phys. Lett. 83 358

[17] Bauer C, Boschloo G, Mukhtar E and Hagfeldt A 2001 J. Phys. Chem. B 105 5585

[18] Zhou J, Xu N S and Wang Z L 2006 Adv. Mater. 18 2432

[19] Ito M 1991 Biomaterials 12 41

[20] Orstavik D and Hongslo J K 1985 Biomaterials 6 129

[21] Kolmakov A, Zhang Y, Cheng G and Moskovits M 2003 Adv. Mater. 15 997

[22] Kolmakov A and Moskovits M 2004 Annu. Rev. Mater. Res. 34 151

[23] Shishiyanu S T, Shishiyanu T S and Lupan O I 2005 Sensors Actuators B 107 379 4 Adv. Nat. Sci.: Nanosci. Nanotechnol. 3 (2012) 035005 R K Sharma et al

[24] Lupan O, Chai G and Chow L 2008 Microelectron. Eng. 85 2220

[25] Lupan O, Chow L, Shishiyanu S, Monaico E, Shishiyanu T, Ontea V S, Roldan Cuenya B, Naitabdi A, Park S and Schulte A 2009 Mater. Res. Bull. 44 63

[26] Lyu S C, Zhang Y, Ruh H, Lee H-J, Shim H-W, Suh E-K and Lee C J 2002 Chem. Phys. Lett. 363 134

[27] Huang M H, Wu Y, Feick H, Tran N, Weber E and Yang P 2002 Adv. Mater. 13 113

[28] Jin B J, Bae S H, Lee S Y and Im S 2000 Mater. Sci. Eng. B 71 301

[29] Issei S and Takeshi K 2003 Appl. Surf. Sci. 216 603

[30] Wu X, Chen H, Gong L, Qu F and Zheng Y 2011 Adv. Nature Sci.: Nanosci. Nanotechnol. 2 035006

[31] Zhao Q X, Klason P, Willander M, Zhong H M, Lu W and Yang J H 2005 Appl. Phys. Lett. 87 211912

[32] Moe B T, Svensson B G, Yu K A, Klason P, Zhao Q X and Willander M 2006 Appl. Phys. Lett. 89 262112

[33] Studenikinm S A, Golegu N and Cocivera M 1998 J. Appl. Phys. 84 2287

[34] Ramachandran, Ashutosh T and Narayan J 2004 Appl. Phys. Lett. 84 5255

[35] Xing G Z et al 2008 Adv. Mater. 20 3521

[36] Zhuge L J, Wu X M, Wu Z F, Chen X M and Meng Y D 2009 Scr. Mater. 60 214

[37] Hong N H, Sakai J, Huong N T, Poirot N and Ruyter A 2005 Phys. Rev. B 72 045336

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